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1 article(s) from Yuan, Mengfei

Remarkable functions of sn-3 hydroxy and phosphocholine groups in 1,2-diacyl-sn-glycerolipids to induce clockwise (+)-helicity around the 1,2-diacyl moiety: Evidence from conformation analysis by ¹H NMR spectroscopy

Yoshihiro Nishida,
Mengfei Yuan,
Kazuo Fukuda,
Kaito Fujisawa,
Hirofumi Dohi and
Hirotaka Uzawa

Beilstein J. Org. Chem. 2017, 13, 1999–2009, doi:10.3762/bjoc.13.196

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Figure 1: (a) Structures of cell-membrane glycerophospholpids with a common asymmetric 1,2-diacyl-sn-glycerol...

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Scheme 1: The four 1,2-dipalmitoyl-sn-glycerols 1–4 examined in this study.

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Figure 2: ¹H NMR spectra of 1,2-dipalmitin (3) in CDCl₃ after partial isomerization into the 1,3-isomer. (a) ...

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Figure 3: Fractional populations (%) of the three staggered conformers around the sn-1,2 C–C single bond in 1...

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Scheme 2: Structures of glycerophospholipids with a common structural skeleton of 1,2-dipalmitoyl-sn-glycerol...

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Figure 4: Partial ¹H NMR spectrum of 4 in a mixture of CDCl₃ and methanol-d₄ (C/M = 10:1, v/v).

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Figure 5: Linear relation between the helical disparity (%) and gt(+) population (%) as observed for the heli...

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Figure 6: An empirical diagram showing helical conformational properties around 1,2-diacyl moiety in asymmetr...

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Scheme 3: Chirally ²H-labelled tripalmitins (1S)- and (1R)-1-[²H]-1 [23].

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Published 25 Sep 2017

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Remarkable functions of sn-3 hydroxy and phosphocholine groups in 1,2-diacyl-sn-glycerolipids to induce clockwise (+)-helicity around the 1,2-diacyl moiety: Evidence from conformation analysis by 1H NMR spectroscopy

Remarkable functions of sn-3 hydroxy and phosphocholine groups in 1,2-diacyl-sn-glycerolipids to induce clockwise (+)-helicity around the 1,2-diacyl moiety: Evidence from conformation analysis by ¹H NMR spectroscopy